Tetrahedron Letters

Convenient synthesis of thiols and disulfides in the polyfluorinated series incorporating a butylic spacer

N Mureau, F Guittard, S Géribaldi

Index: Mureau, Natacha; Guittard, Frederic; Geribaldi, Serge Tetrahedron Letters, 2000 , vol. 41, # 16 p. 2885 - 2889

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Citation Number: 13

Abstract

New fluorinated thiols RF (CH2) pSH and disulfides [RF (CH2) pS] 2 containing a butylic spacer (p= 4) between the perfluorinated part and the thiol (or disulfide) function were easily obtained in good yields with a purity higher than 98%. This allows us to obtain homologues (p> 4) for their use as synthetic intermediates or as constituents for molecular organized systems.