Journal of chemical crystallography

Synthesis and X-ray structure of new 5-amino-methyl-4-isoxazolecarboxylic acid azides

S Ryng, Z Machoń, T Głowiak

Index: Ryng, Stanislaw; Machon, Zdzislaw; Glowiak, Tadeusz Journal of Chemical Crystallography, 1994 , vol. 24, # 8 p. 483 - 488

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Citation Number: 10

Abstract

Abstract The syntheses of the new heterocyclic azides which open a number ways of obtaining interesting isoxazole derivatives has been described. Chemical, spectral and X- ray data giving the evidence of the structure of these compounds are presented. X-ray studies were carried out on compounds I, II (C 5 H 5 N 5 O 2, C 12 H 9 N 5 O 3) with a= 3.775 (2), 7.179 (3); b= 11.593 (3), 8.135 (3); c= 8.443 (3), 11.610 (3); Z= 2, 2 and space ...