Synthesis and Nuclear Magnetic Resonance Spectra of Some 1-Halo-1-iodoalkanes
RC Neuman Jr, ML Rahm
Index: Neumann,R.C.; Rahm,M.L. Journal of Organic Chemistry, 1966 , vol. 31, p. 1857 - 1859
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Citation Number: 18
Abstract
The previously unknown symmetrical dihalides 1, l-diiodopropane and l, l-diiodo-2- methylpropane, have been synthesized by treatment of the corresponding diazoalkane with iodine. The new asymmetrical dihalides, 1-chloro-1-iodopropane and 1-bromo-1- iodopropane, have been obtained by halodecarboxylation of a-chlorobutyric and a- bromobutyric acid, respectively, with lead tetraacetate in the presence of iodine. Nmr ...
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