Thiophenophane-metal complexes. I. Preparation, X-ray structure, and cyclic voltammetry of 2, 5, 8-trithia [9](2, 5) thiophenophane, L, and of its metalcomplexcation …

…, L Shuang, MJ Newlands, JP Charland…

Index: Lucas, C. Robert; Shuang, Liu; Newlands, Michael J.; Charland, Jean-Pierre; Gabe, Eric J. Canadian Journal of Chemistry, 1988 , vol. 66, p. 1506 - 1512

Full Text: HTML

Citation Number: 27

Abstract

Preparation of the thiophenophane C10H14S4,(L), and syntheses of its copper (I) complex [CuL2] ClO4 or [CuL2] BF4 are described. The 13C and 1H nmr spectra of L and the ir spectra (4000-200 cm-1) of [CuL2] ClO4 and [CuL2] BF4 are reported. The molecular ...