Vinyl aromatic compounds. I. The vapor phase dehydration of arylmethylcarbinols

DT Mowry, M Renoll, WF Huber

Index: Mowry; Renoll; Huber Journal of the American Chemical Society, 1946 , vol. 68, p. 1105,1107

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Citation Number: 112

Abstract

June, 1946 VAPOR PHASE DEHYDRATION OF ARYLMETHYLCARBINOLS 1105 bined solution was distilled under reduced pressure. The major part of the charge distilled at 130- 150" at 3 mm. and crystallized on cooling. Recrystallitation from alcohol gave colorless product, mp 76-77, which was identified as tetraethyl ethanetetracarboxylate. Further distillation of the residue after the removal of the above fraction yielded 25 g. of a yellow ...