Tetrahedron: Asymmetry

Synthesis of chiral non-racemic azetidines by lipase-catalysed acetylations and their transformation into amino alcohols: precursors of chiral catalysts

G Guanti, R Riva

Index: Guanti, Giuseppe; Riva, Renata Tetrahedron Asymmetry, 2001 , vol. 12, # 4 p. 605 - 618

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Citation Number: 29

Abstract

Azetidinic mono-acetate 7, diol 6b and di-acetate 10a were prepared with high ee using PPL- catalysed acetylations. The absolute configurations of all new enantioenriched compounds were assigned by chemical correlation with known compounds. Mono-acetate 7 was then transformed into 30, an amino alcohol of noteworthy potential interest since it represents an interesting precursor for chiral catalysts, such as 32.

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