Journal of the American Chemical Society

Dimethylcarbamyldimethylthiocarbamyl Disulfide

EC Gregg Jr

Index: Gregg Journal of the American Chemical Society, 1952 , vol. 74, p. 3691

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Citation Number: 10

Abstract

sample of 20 g.(0.096 mole) of bis-(dimethylthiocarbamyl) sulfide'was dissolved in 200 ml. of benzene. To this solu-tion at room temperature was added with stirring over a five-minute period a solution of 38.4 g.(0.48 gram-atom) of bromine in 100 ml. of carbon tetrachloride. A deep orange solid precipitated immediately. The stirring was continued until a uniform suspension was obtained. The insoluble orange colored DreciDitate was filtered off and ...