A Method for the Synthesis of Certain 2-Substituted Phenanthrenes

B Riegel, MH Gold, MA Kubico

Index: Riegel; Gold; Kubico Journal of the American Chemical Society, 1942 , vol. 64, p. 2221

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Abstract

~-(4-Chlorophenyl)-2, 6-dichlorophenol (XI).-The impure 4-(4-chlorophenyl)-2, 6- dichlorophenol was prepared according to the method of Colbert, Meigs and Mackin. lo This was crystallized several times from carbon tetrachloride, thus yielding the pure compound with a constant melting point of 144".(A 9% yield was obtained.) When a melting point was taken on a mixture of this compound with the chlorophenylphenol obtained from 111 it ...