The Journal of Organic Chemistry

Properties and reactions of 1-methyl-3-phospholanone 1-oxide

LD Quin, RC Stocks

Index: Quin,L.D.; Stocks,R.C. Journal of Organic Chemistry, 1974 , vol. 39, p. 686 - 690

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Citation Number: 11

Abstract

C, 61.43; H, 10.00; P, 11.17. Diethyl p-methanyl-2, s-diphosphonate (12): glc 2.5% 12a, 45.5% 12b, 45.9% 12c, 6% 12d; d24= 1.0894, n250 1.4676, a%+ 4.9'; ir 3440, 2890, 1430, 1380, 1230, 1155, 1090, 1045, 1020, 942, 823, 784 cm-l; nmr 6 1.04 (d, 6, J= 6 Hz, C~ JO- CH~), 1.34 (t, 12,