Journal of the American Chemical Society

THE ACTION OF ALKYL CHLOROCARBONATES ON AMINO-ARYLARSONIC ACIDS1

CS Hamilton, C Sly

Index: Hamilton; Sly Journal of the American Chemical Society, 1925 , vol. 47, p. 437

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Citation Number: 4

Abstract

Following the procedure of Roselo the alcohol used was placed in a slender glass cylinder and cooled to 5'. Phosgene, first dried by passing through concd. sulfuric acid, was then passed in a slow stream through the cold alcohol. When the reaction was complete, as indicated by the fact that the phosgene bubbled through the alcohol unchanged, the reaction mixture was transferred to a separatary funnel and washed several times in ice water. This ...