Organic preparations and procedures international

Synthesis of substituted 1-tetralones

P Kumar

Index: Kumar, Punit Organic Preparations and Procedures International, 1997 , vol. 29, # 4 p. 477 - 480

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Citation Number: 22

Abstract

Volume 29, No. 4, 1997 OPPI BRIEFS 50 psi followed by hydrolysis gave the acid 8. Compound 8 was treated with polyphosphoric ester (PPE)'in CHCl, at room temperature to give 2 (77.8% overall yield) along with 8-methoxy-ltetralone (9)(8%). Similarly, benzyl chloride (10) was converted into 1-tetralone (3)(overall yield 77%). The synthesis of 5, 6- dimethoxy-1-tetralone (4)(overall yield 67%) was also completed by the above approach ...