Inorganic chemistry

Kinetic and Mechanistic Aspects of Sulfur Recovery from Pd2I2 (μ-S)(μ-dpm) 2 Using I2 and Structures of Pd (II) Complexes with the Chelated Monosulfide of dpm

TYH Wong, SJ Rettig, BR James

Index: Carmalt, Aire J.; Cowley, Alan H.; Decken, Andreas; Lawson, Yvonne G.; Norman, Nicholas C. Acta Crystallographica Section C: Crystal Structure Communications, 1996 , vol. 52, # 4 p. 931 - 933

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Citation Number: 26

Abstract

... The solution was stirred for 1 h before MeOH (25 mL) was added to precipitate a red-brown solid that was filtered off, washed with MeOH (2 × 10 mL), and dried in vacuo. Yield: 0.16 g (80%). 1 H NMR (20 °C, CDCl 3 ): δ 7.0−8.0 m (40H, Ph), δ 4.98 dt (1H, CH 2 , J HH = 12 ...