Journal - Association of Official Analytical Chemists 1987-01-01

Titrimetric determination of iodine-bromine numbers of some edible oils using three N-chloroimides.

N Jayasree, P Indrasenan

Index: J. Assoc. Off. Anal. Chem. 70(4) , 762-3, (1987)

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Abstract

Three simple titrimetric methods have been developed to determine iodine-bromine numbers of some edible oils, such as coconut, gingelly, groundnut, mustard, olive, palm olein, and sunflower, using 3 N-chloroimides. The 3 N-chloroimides are N-chlorophthalimide, N-chlorosuccinimide, and N-chlorosaccharin, all of which have recently been developed as potential oxidimetric titrants for use in aqueous acetic acid medium. The proposed excess back-titration methods have advantages over existing methods in terms of ease of extraction into aqueous acetic acid layer, shorter reaction time of NCSA method, and stability of N-chloroimides in solid state.