Phosphane–Tetrahalodiborane (4) Adducts: Formation of closo??3, 4, 5, 6??Tetrabromo??1, 2??diphosphahexaborane (4)

W Keller, LG Sneddon, W Einholz…

Index: Chemische Berichte, , vol. 125, # 11 p. 2343 - 2346

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Citation Number: 17

Abstract

... mmol) of 4a which was heated at 450°C for 6 h in an evacuated, sealed pyrex tube of 20 ml volume showed, as ... Ber. 1992, 125, 2343 - 2346 ... The undissolved orange powder was filtrated off and dried in vacuo (yield 0.15 g). - Elementary analysis: Found B 4.56, Br 41.46, P 46.79 ...