The Journal of Organic Chemistry

Organic Disulfides and Related Substances. XVI. Synthesis of Bisthiolsulfonates1a-d

L Field, WB Lacefield

Index: Field,L.; Lacefield,W.B. Journal of Organic Chemistry, 1966 , vol. 31, p. 599 - 601

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Citation Number: 6

Abstract

2AcNH (CHz) zSH+ 4n-CdHsONO+ HOzS (CH2) 4SOzH (3) The first route, and in this instance perhaps the more effective, involves thioalkylation of a sulfinate salt by a thiolsulfonate (eq. 2). The interchange equilibrium on which it is based (eq. 4) has been studied