Australian Journal of Chemistry

Sodium benzyloxycarbonyl thiosulphate: a water-soluble acylating reagent

JB Caldwell, R Ledger, B Milligan

Index: Caldwell,J.B. et al. Australian Journal of Chemistry, 1966 , vol. 19, p. 1297 - 1298

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Citation Number: 6

Abstract

Reaction of Sodium Benzyloxycarbonyl Thiosulphate with Thiols (i) Equimolar proportions of sodium benzyloxycarbonyl thiosulphate and naphthalene-2-thiol were stirred in aqueous suspension at pH 9 for 2 hr, giving 2, 2'-dinaphthyl disulphide (92%), plates (from chloroform), mp 142'(lit. 4 mp 139"). An authentic sample of benzyloxycarbonyl 2-naphthyl sulphide was prepared by treating naphthalene-2-thiol with benzyloxycarbonyl chloride in ...

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