Organic preparations and procedures international

SYNTHESIS OF METHOXYTAMOXIFEN

HA El-Wakil

Index: El-Wakil, Hoda A. Organic Preparations and Procedures International, 1991 , vol. 23, # 6 p. 754 - 757

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Abstract

OW1 BRIEFS Volume 23, No. 6 (1991)(sept, 2H, 2 x-CH (C&) J, 6.8 (s, 4H, aromatic). The alkaline layer was acidified with conc. HCl and extracted with petroleum ether (3 x 60 ml). The organic layer was washed with water, brine, dried (N% SOJ. Removal of solvent and the distillation of the residue furnished a pale yellow oil (2.89, 63%) of O-isopropoxyphenol (3),'bp. 130/4 mm, lit. I bp. 100-102/11 mm. lR (neat) 3560, 3000.1610, 1510, 1480, 1400, ...