The total synthesis of neoamphimedine

DV LaBarbera, TS Bugni…

Index: Nakahara, Shinsuke; Tanaka, Yoshihiro; Kubo, Akinori Heterocycles, 1996 ,  vol. 43,  # 10  p. 2113 - 2123

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Citation Number: 17

Abstract

... mixture was then heated at 50 °C for 1 h, diluted with an equal volume of ethyl ... C under argon for 2 h. The reaction was cooled to room temperature, poured into 10 mL of ... Recrystallization with ethyl acetate and hexanes gave pale orange needles (43 mg, 80% yield): mp >162 °C ...