(14) Anal. Calcd for CloH1806Ru: C, 35.82; H, 5.41. Found: C, 35.64; H. 5.29. .~. . (15) 6 crystallizes in s ace group P2,2,2, (P2,; No. 19) with u = 7.8085 (12) A, b = 8.0452 (IO) ,f, c = 19.2704 (28) A, V = 1210.6 (3) A3, and = 1.840 g cm-3 for Z = 4, T = 183 K. The structure was solved via an automatic Patterson method (SHELXTL PLUS). Refinement of positional and anisotropic thermal parameters led to convergence with RF = 2.276, R,, = 2.72, and GOF = 1.04 for 156 ...
