SYNTHESIS OF PERCHLOROFULVALENE1

ET McBee, CW Roberts, JD Idol Jr

Index: McBee; Idol; Roberts Journal of the American Chemical Society, 1955 , vol. 77, p. 4942

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Citation Number: 7

Abstract

121”(111)(Amax 330 mp, E 2950)) by cuprous chloride coupling of hexachlorocyclopentadiene. 6 Compound I11 was reduced over platinum to give bicyclopentyl, bp 188-190') nZo~ 1.4650. On being heated to 250”) I11 lost a mole of chlorine giving compound IV (85y0), mp 347”. Anal. Calcd. for CloClg: C, 29.70; C1, 70.30; mol. wt.,