The Journal of Organic Chemistry

Some novel sulfonamides. Chlorosulfonation of aryl alkyl sulfides

AH Goldkamp

Index: Goldkamp,A.H. Journal of Organic Chemistry, 1969 , vol. 34, # 6 p. 1780 - 1785

Full Text: HTML

Citation Number: 3

Abstract

The chlcrrosulfonation of three methylthio-substituted benzenes has been investigated. With two of the compounds, the reaction proved satisfactory for preparation of sulfonamide derivatives. In the more favorable case, 2, 4dimethylthioacetanilide readily gave a crystalline sulfonyl chloride. Subsequent oxidation gave the corresponding disulfones. Various tetrasubstituted compounds were readily characterized by bands for isolated aromatic ...