A new preparative route to organic halides from alcohols via the reduction of polyhalomethanes

E Léonel, JP Paugam, JY Nédélec

Index: Journal of Organic Chemistry, , vol. 62, # 20 p. 7061 - 7064

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Citation Number: 18

Abstract

... The combined organic layers were washed with water, dried over MgSO4, and concentrated. Products were isolated by column chromatography (silica gel, 70-230 mesh; eluent pentane). ... Scheme 2 Notes J. Org. Chem., Vol. 62, No. 20, 1997 7063 Page 4. -0.2 V/SCE. ...