Applying novel and efficient method, new tris (triorganosilyl) phosphites were synthesized and further used for the preparation of new well-defined platinum complexes [Pt (DVTMDS){P (OSiR3) 3}](DVTMDS=(H2CCHSiMe2) 2O, R3= Si7O9 (iOct) 7, iPr3, MePh2, Ph3,(OtBu) 3,(OSiMe3) 3) which were well characterized by spectroscopic methods. Structures of two platinum (0) complexes,[Pt {η4-(H2CCHSiMe2) 2O}{P (OSiPh3) 3}](10) ...