e.g. Filippa Pettersson or Cancer Res. 75(6) , 1102-12, (2015) or 10.1002/anie.201600521
Enzymic synthesis and biochemical activity of various indazole adenine dinucleotides
S Tono-oka, Y Tone, V E. Marquez…
Index: Witt; Noelting; Grandmougin Chemische Berichte, 1892 , vol. 25, p. 3156 Full Text Show Details Tono-Oka; Tone; Marquez; et al. Bulletin of the Chemical Society of Japan, 1985 , vol. 58, # 1 p. 309 - 315
Each of 5-or 6-amino-, acetamido-, hydroxy-, methoxy-, and chloroindazoles (including an unsubstituted one) and β NAD were subjected to an NADase-catalyzed base-exchange reaction to produce a corresponding title compound with a 41–76% yield. A difficulty, due to the poor solubility in water of indazole bases, was overcome by the addition of DMSO (∼ 20%) without a remarkable decrease in NADase activity. In most cases, the obtained ...