NMR spectra of a hydrocarbon-soluble organosodium compound and its lithium analogs

NI Pakuro, AA Arest-Yakubovich, LV Shcheglova…

Index: Pakuro; Arest-Yakubovich; Shcheglova; Petrovsky; Chekulaeva Russian Chemical Bulletin, 1996 , vol. 45, # 4 p. 838 - 840

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Citation Number: 10

Abstract

Abstract 1 H, 23 Na, and 7 Li NMR spectra of 2-ethyl hexylsodiurn, 2-ethylhexyllithium, and isobutyllithium obtained in the reaction of the corresponding alkyl chlorides and metals have been recorded. The 1 HN MR signal for the protons of the CH 2 Na group is shifted upheld compared with that for the protons of the CH 2 Li group (doublets at δ-0.88 and δ-0.83, respectively). The composition of the products of reaction of 2-ethylhexyl chloride with ...