The Journal of Organic Chemistry

Direct perfluoroalkylation including trifluoromethylation of aromatics with perfluoro carboxylic acids mediated by xenon difluoride

Y Tanabe, N Matsuo, N Ohno

Index: Tanabe, Yoo; Matsuo, Noritada; Ohno, Nobuo Journal of Organic Chemistry, 1988 , vol. 53, # 19 p. 4582 - 4585

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Citation Number: 82

Abstract

The" 0 NMR spectra were obtained with a Bruker WP 200 SY multinuclear spectrometer operating at 27.1 MHz for 170. No field/frequency locking system was used, and the spectra were obtained at about 30" C. Chemical shifts were measured relative to acetone as external reference. The acetone chemical shift (+ 572 ppm from water) was previously determined in a separate experiment.