Tetrahedron letters

Silicon modified reduction and reductive alkylation-application to the phenanthrene system

PW Rabideau, Z Marcinow

Index: Rabideau, Peter W.; Marcinow, Zbigniew Tetrahedron Letters, 1988 , vol. 29, # 31 p. 3761 - 3764

Full Text: HTML

Citation Number: 12

Abstract

Download full text in PDF Opens in a new window. Article suggestions will be shown in a dialog on return to ScienceDirect. ... Please enable JavaScript to use all the features on this page. ... A trimethylsilyl (TMS) substituent is used to control the metal-ammonia reduction of phenanthrenes. The TMS group is then removed by tetrabutylammonium fluoride (TBAF) and replaced by either H or R.' ... A trimethylsilyl group is used to control metal-ammonia ...

 Related Synthetic Route
N/A Structure

119406-13-2

N/A

Ethyl iodide Structure

75-03-6

Ethyl iodide

~21%

9-methyl-9,10-dihydrophenanthrene Structure

52978-94-6

9-methyl-9,10-d...

N/A Structure

119406-15-4

N/A

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9,10-dihydrophenanthrene Structure

56465-93-1

9,10-dihydrophe...

methyl iodide Structure

74-88-4

methyl iodide

~89%

9,10-Dihydrophenanthrene Structure

776-35-2

9,10-Dihydrophe...

9-methyl-9,10-dihydrophenanthrene Structure

52978-94-6

9-methyl-9,10-d...

Learn More
N/A Structure

119406-13-2

N/A

methyl iodide Structure

74-88-4

methyl iodide

~8%

9-methyl-9,10-dihydrophenanthrene Structure

52978-94-6

9-methyl-9,10-d...

(9S,10S)-9,10-dimethyl-9,10-dihydrophenanthrene Structure

22140-65-4

(9S,10S)-9,10-d...

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N/A Structure

119406-13-2

N/A

~%

9-methyl-9,10-dihydrophenanthrene Structure

52978-94-6

9-methyl-9,10-d...

Learn More

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