... The chemical shifts were reported per million (8, ppm) downfield from tetram- ethylsilane (TMS) which was used as internal standard. ... Chenu, 24,994 (1981). [6] G. Coudert, С. Borredon-Watrin and G. Guillaumet, J. Heterocyclic Chem., 24, 609 (1987). ...