Hydrodehalogenation of alkyl iodides with base-mediated hydrogenation and catalytic transfer hydrogenation: application to the asymmetric synthesis of N-protected α …

PK Mandal, JS Birtwistle…

Index: Kohno, Harumichi; Iwakuma, Takeo; Yamada, Koichiro Synthetic Communications, 1998 , vol. 28, # 11 p. 1935 - 1945

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Abstract

... After 3 h, the volume of the solution was reduced under reduced pressure to ca ... Identical to that reported by Quagliato et al.(11) and Caputo et al.(22) 1 H NMR (300 MHz, CDCl 3 ) δ 1.45 ... HRMS (ESI-TOF) m/z:[M + NH 4 ] + Calcd for C 24 H 28 IN 2 O 3 519.1145; Found 519.1154 ...