Synthesis, 15 N NMR spectra and GIAO calculated data of the seven positional isomers of 15 N-labeled N, N-dimethylsulfamoylquinoline

…, A Maślankiewicz, MJ Maślankiewicz…

Index: Marciniec, Krzysztof; Maslankiewicz, Andrzej; Maslankiewicz, Maria J.; Kurczab, Rafal Journal of Molecular Structure, 2012 , vol. 1015, p. 46 - 50

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Citation Number: 2

Abstract

The one-step synthesis of positional isomers of N, N-dimethylsulfamoylquinoline are presented. Seven newly synthesized compounds have been characterized by elemental analyses, MS, 1H and 15N NMR spectral data. The long-range correlations between the ring protons and the endocyclic nitrogen atoms were observed in the gHMBC experiments. The spectral positions of the nitrogen atoms from the sulfonamide groups were drawn from the ...