Continuous-Flow Preparation and Use of β-Chloro Enals Using the Vilsmeier Reagent

L Pellegatti, SL Buchwald

Index: Organic Process Research and Development, , vol. 16, # 8 p. 1442 - 1448

Full Text: HTML

Citation Number: 11

Abstract

... The combined organic phases were then washed with water (3 × 50 mL) and then brine (30 mL ... Using the reaction setup as depicted in Scheme 3 and the General procedure A for the ... The vessel was evacuated and backfilled with argon (this process was repeated a total of three ...