Download PDF Opens in a new window. Article suggestions will be shown in a dialog on return to ScienceDirect. ... Please enable JavaScript to use all the features on this page. ... A new series of BINOL-based macrocycles with two phenolic protons have been synthesized via oxidative coupling reaction using CuCl(OH)–TMEDA. ... Reagents and conditions: (i) NaOH, n-BuOH, reflux, 2d; (ii) TsCl, NaOH, THF–H2O ... Reagents and conditions: (i) NaOH, n-BuOH, ...