Nitration of 4-acetylamino-4'-nitrodiphenyl sulfide

…, GV Kiseleva, SL Kuznetsova, AN Mikhailyuk

Index: Pilyugin; Valitov; Kiseleva; Kuznetsova; Mikhailyuk Russian Journal of General Chemistry, 2003 , vol. 73, # 2 p. 244 - 248

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Abstract

Abstract Procedures have been developed for the acylation of 4-amino-4'-nitrodiphenyl sulfide with an almost quantitative yield by the action of acetic anhydride in aprotic organic solvents and subsequent nitration of 4-acetylamino-4'-nitrodiphenyl sulfide with nitric acid in a mixture of acetic acid and an aprotic organic solvent with addition of a mixture of sulfuric and acetic acids by the end of the process.