Organometallics

X-ray crystal and molecular structure of bis (biphenylyl-2) tin (IV) dichloride, a discrete, molecular, organotin chloride

JL Baxter, EM Holt, JJ Zuckerman

Index: Baxter, J. L.; Holt, E. M.; Zuckerman, J. J. Organometallics, 1985 , vol. 4, p. 255 - 259

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Citation Number: 16

Abstract

Bis (biphenylyl-2) tin (IV) dichloride forms clear, diamond-shaped, monoclinic crystals, mp 165-166" C, in the space roup P2, ln with a= 13.039 (5) A, b= 14.173 (4) A, c= 11.478 (4) A,/3= 90.83 (3) O, V= on a Syntex P3 automated diffractometer with monochromatic Mo Ka radiation (X,= 0.71069 A) and refined to afii R value of 5.0% for the 2754 reflections included in the least-squares sums. The monomeric molecules are well separated in space with the ...