Abstract The reaction whereby aldose or ketose precursors are converted in acidified aqueous ethanol in the presence of p-toluidine into 3-deoxyaldos-2-uloses and the latter are trapped as the crystalline bis (benzoylhydrazones) is shown to be of wide generality. Sugar precursors having four-, five-, six-, and seven-carbon chains, and aroylhydrazines having the p-toluoyl, p-anisoyl, p-chlorobenzoyl, p-iodobenzoyl, or p-nitrobenzoyl groups, all ...