Efficient Preparative-Scale Procedures for the Pd-Catalyzed Methoxycarbonylation of Acetylenes

SF Vasilevsky, BA Trofimov, AG Mal'kina…

Index: Synthetic Communications, , vol. 24, # 1 p. 85 - 88

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Citation Number: 18

Abstract

SYNTHETIC COMMUNICATIONS, 24(1), 85-88 (1994) ... Optimal yields were obtained from the reaction at 15°C. At 10°C the conversion proceeded much more slowly, while yields significantly decreased (to below 40 %) when performing ... (1 3.4 g) of anhydrous copper(I1)chloride. ...