Tetrahedron

An approach to triquinane synthesis using the Pauson–Khand reaction

…, C Hirosawa, P Schmidt, KA Abboud, N L'Helias

Index: Krafft, Marie E.; Kyne, Graham M.; Hirosawa, Chitaru; Schmidt, Peter; Abboud, Khalil A.; L'Helias, Nathalie Tetrahedron, 2006 , vol. 62, # 50 p. 11782 - 11792

Full Text: HTML

Citation Number: 12

Abstract

Download PDF Opens in a new window. Article suggestions will be shown in a dialog on return to ScienceDirect. ... Please enable JavaScript to use all the features on this page. ... Tricyclic skeletons have been generated from acyclic enyne precursors by using an intramolecular Pauson–Khand reaction in combination with aldol, Michael and alkylation reactions. ... The goal of this study was a one-pot synthesis of tricycles using Pauson–Khand reactions followed ...

 Related Synthetic Route
1-[tert-butyl(dimethyl)silyl]oxy-9-trimethylsilylnon-8-yn-4-ol Structure

917989-34-5

1-[tert-butyl(d...

~96%

1-[tert-butyl(dimethyl)silyl]oxy-9-trimethylsilylnon-8-yn-4-one Structure

917989-60-7

1-[tert-butyl(d...

5-bromopent-1-ynyl(trimethyl)silane Structure

66927-74-0

5-bromopent-1-y...

~%

1-[tert-butyl(dimethyl)silyl]oxy-9-trimethylsilylnon-8-yn-4-one Structure

917989-60-7

1-[tert-butyl(d...

4-(tert-Butyldimethylsilyloxy)butanal Structure

87184-81-4

4-(tert-Butyldi...

~%

1-[tert-butyl(dimethyl)silyl]oxy-9-trimethylsilylnon-8-yn-4-one Structure

917989-60-7

1-[tert-butyl(d...

acetic acid 6-(tert-butyldiphenylsilanyloxy)-2-hydroxy-hexyl ester Structure

917989-44-7

acetic acid 6-(...

~80%

[6-[tert-butyl(diphenyl)silyl]oxy-2-oxohexyl] acetate Structure

917989-63-0

[6-[tert-butyl(...

6-[tert-butyl(diphenyl)silyl]oxyhexane-1,2-diol Structure

91898-18-9

6-[tert-butyl(d...

~%

[6-[tert-butyl(diphenyl)silyl]oxy-2-oxohexyl] acetate Structure

917989-63-0

[6-[tert-butyl(...

5-bromopent-1-ynyl(trimethyl)silane Structure

66927-74-0

5-bromopent-1-y...

4-(tert-Butyldimethylsilyloxy)butanal Structure

87184-81-4

4-(tert-Butyldi...

~56%

1-[tert-butyl(dimethyl)silyl]oxy-9-trimethylsilylnon-8-yn-4-ol Structure

917989-34-5

1-[tert-butyl(d...

9-((1,1-dimethylethyl)dimethylsilyloxy)-6-methylene-1-trimethylsilylnon-1-yne Structure

917989-61-8

9-((1,1-dimethy...

~47%

4-methylidenenon-8-yn-1-ol Structure

917989-35-6

4-methylideneno...

1-[tert-butyl(dimethyl)silyl]oxy-9-trimethylsilylnon-8-yn-4-ol Structure

917989-34-5

1-[tert-butyl(d...

~%

4-methylidenenon-8-yn-1-ol Structure

917989-35-6

4-methylideneno...

1-[tert-butyl(dimethyl)silyl]oxy-9-trimethylsilylnon-8-yn-4-one Structure

917989-60-7

1-[tert-butyl(d...

~%

4-methylidenenon-8-yn-1-ol Structure

917989-35-6

4-methylideneno...

5-bromopent-1-ynyl(trimethyl)silane Structure

66927-74-0

5-bromopent-1-y...

~%

4-methylidenenon-8-yn-1-ol Structure

917989-35-6

4-methylideneno...

4-methylidenenon-8-yn-1-ol Structure

917989-35-6

4-methylideneno...

~70%

4-methylidenenon-8-ynal Structure

917989-36-7

4-methylideneno...

1-[tert-butyl(dimethyl)silyl]oxy-9-trimethylsilylnon-8-yn-4-ol Structure

917989-34-5

1-[tert-butyl(d...

~%

4-methylidenenon-8-ynal Structure

917989-36-7

4-methylideneno...

1-[tert-butyl(dimethyl)silyl]oxy-9-trimethylsilylnon-8-yn-4-one Structure

917989-60-7

1-[tert-butyl(d...

~%

4-methylidenenon-8-ynal Structure

917989-36-7

4-methylideneno...

9-((1,1-dimethylethyl)dimethylsilyloxy)-6-methylene-1-trimethylsilylnon-1-yne Structure

917989-61-8

9-((1,1-dimethy...

~%

4-methylidenenon-8-ynal Structure

917989-36-7

4-methylideneno...

5-bromopent-1-ynyl(trimethyl)silane Structure

66927-74-0

5-bromopent-1-y...

~%

4-methylidenenon-8-ynal Structure

917989-36-7

4-methylideneno...

4-methylidenenon-8-yn-1-ol Structure

917989-35-6

4-methylideneno...

tert-Butyldimethylsilyl chloride Structure

18162-48-6

tert-Butyldimet...

~89%

tert-butyl-dimethyl-(4-methylidenenon-8-ynoxy)silane Structure

917989-37-8

tert-butyl-dime...

1-[tert-butyl(dimethyl)silyl]oxy-9-trimethylsilylnon-8-yn-4-ol Structure

917989-34-5

1-[tert-butyl(d...

~%

tert-butyl-dimethyl-(4-methylidenenon-8-ynoxy)silane Structure

917989-37-8

tert-butyl-dime...

1-[tert-butyl(dimethyl)silyl]oxy-9-trimethylsilylnon-8-yn-4-one Structure

917989-60-7

1-[tert-butyl(d...

~%

tert-butyl-dimethyl-(4-methylidenenon-8-ynoxy)silane Structure

917989-37-8

tert-butyl-dime...

9-((1,1-dimethylethyl)dimethylsilyloxy)-6-methylene-1-trimethylsilylnon-1-yne Structure

917989-61-8

9-((1,1-dimethy...

~%

tert-butyl-dimethyl-(4-methylidenenon-8-ynoxy)silane Structure

917989-37-8

tert-butyl-dime...

5-bromopent-1-ynyl(trimethyl)silane Structure

66927-74-0

5-bromopent-1-y...

~%

tert-butyl-dimethyl-(4-methylidenenon-8-ynoxy)silane Structure

917989-37-8

tert-butyl-dime...

Vinylmagnesium bromide Structure

1826-67-1

Vinylmagnesium ...

4-(tert-Butyldimethylsilyloxy)butanal Structure

87184-81-4

4-(tert-Butyldi...

Ethyl chloroformate Structure

541-41-3

Ethyl chloroformate

~67%

[6-[tert-butyl(dimethyl)silyl]oxy-3-ethenylhexan-2-yl] carbonate Structure

917989-50-5

[6-[tert-butyl(...

[6-[tert-butyl(dimethyl)silyl]oxy-3-ethenylhexan-2-yl] carbonate Structure

917989-50-5

[6-[tert-butyl(...

~83%

[6-[tert-butyl(dimethyl)silyl]oxy-3-formylhexan-2-yl] carbonate Structure

917989-51-6

[6-[tert-butyl(...

4-(tert-Butyldimethylsilyloxy)butanal Structure

87184-81-4

4-(tert-Butyldi...

~%

[6-[tert-butyl(dimethyl)silyl]oxy-3-formylhexan-2-yl] carbonate Structure

917989-51-6

[6-[tert-butyl(...


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