Liebigs Annalen der Chemie

1??Substituierte 3??Phenyl??1, 2, 4??triazol??5??carbaldehyde

D Moderhack

Index: Moderhack, Dietrich Liebigs Annalen der Chemie, 1984 , # 1 p. 48 - 65

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Citation Number: 0

Abstract

Abstract Die Aldehyde 7, erste Vertreter der noch unbekannten Klasse 1-substituierter 1, 2, 4- Triazol-5-carbaldehyde, sind in sehr guter Ausbeute durch Bleitetraacetatoxidation der Alkohole 2 zugänglich; ein alternativer Weg besteht in der Anwendung der Kröhnke- Reaktion auf 5. Als Folge des stärkeren Elektronenzugs des Triazol-5-yl-Systems A gegenüber dem System B unterliegen die Verbindungen 7—anders als die isomeren 3- ...

 Related Synthetic Route
Piperidine Structure

110-89-4

Piperidine

~%

1-[(2-methyl-5-phenyl-1,2,4-triazol-3-yl)-piperidin-1-ylmethyl]piperidine Structure

89060-82-2

1-[(2-methyl-5-...

2-phenyl-2-oxazolin-4-one Structure

30216-01-4

2-phenyl-2-oxaz...

~%

1-[(2-methyl-5-phenyl-1,2,4-triazol-3-yl)-piperidin-1-ylmethyl]piperidine Structure

89060-82-2

1-[(2-methyl-5-...

1-Methyl-3-phenyl-1H-1,2,4-triazole-5-carbaldehyde Structure

89060-36-6

1-Methyl-3-phen...

~%

1-[(2-methyl-5-phenyl-1,2,4-triazol-3-yl)-piperidin-1-ylmethyl]piperidine Structure

89060-82-2

1-[(2-methyl-5-...

N/A Structure

26254-15-9

N/A

~%

1-[(2-methyl-5-phenyl-1,2,4-triazol-3-yl)-piperidin-1-ylmethyl]piperidine Structure

89060-82-2

1-[(2-methyl-5-...

(2-methyl-5-phenyl-2H-[1,2,4]triazol-3-yl)-methanol Structure

26254-08-0

(2-methyl-5-phe...

~%

1-[(2-methyl-5-phenyl-1,2,4-triazol-3-yl)-piperidin-1-ylmethyl]piperidine Structure

89060-82-2

1-[(2-methyl-5-...

Piperidine Structure

110-89-4

Piperidine

(2-Methyl-5-phenyl-2H-[1,2,4]triazol-3-yl)-piperidin-1-yl-methanol Structure

89060-75-3

(2-Methyl-5-phe...

~%

1-[(2-methyl-5-phenyl-1,2,4-triazol-3-yl)-piperidin-1-ylmethyl]piperidine Structure

89060-82-2

1-[(2-methyl-5-...

3-(nitrosomethylidene)-2,5-diphenyl-1H-1,2,4-triazole Structure

89060-49-1

3-(nitrosomethy...

~89%

2,5-diphenyl-1,2,4-triazole-3-carbonitrile Structure

89060-50-4

2,5-diphenyl-1,...

2-phenyl-2-oxazolin-4-one Structure

30216-01-4

2-phenyl-2-oxaz...

~%

2,5-diphenyl-1,2,4-triazole-3-carbonitrile Structure

89060-50-4

2,5-diphenyl-1,...

2,5-diphenyl-1,2,4-triazole-3-carbaldehyde Structure

89060-38-8

2,5-diphenyl-1,...

~%

2,5-diphenyl-1,2,4-triazole-3-carbonitrile Structure

89060-50-4

2,5-diphenyl-1,...

Phenylhydrazine Structure

100-63-0

Phenylhydrazine

~%

2,5-diphenyl-1,2,4-triazole-3-carbonitrile Structure

89060-50-4

2,5-diphenyl-1,...

(1,3-diphenyl-1H-1,2,4-triazol-5-yl)methanol Structure

26254-07-9

(1,3-diphenyl-1...

~%

2,5-diphenyl-1,2,4-triazole-3-carbonitrile Structure

89060-50-4

2,5-diphenyl-1,...

2-phenyl-2-oxazolin-4-one Structure

30216-01-4

2-phenyl-2-oxaz...

4-Methylphenylhydrazine Structure

539-44-6

4-Methylphenylh...

~89%

[2-(4-methylphenyl)-5-phenyl-1,2,4-triazol-3-yl]methanol Structure

89060-23-1

[2-(4-methylphe...

[2-(4-nitro-phenyl)-5-phenyl-2H-[1,2,4]triazol-3-yl]-methanol Structure

26254-22-8

[2-(4-nitro-phe...

~90%

5-(chloromethyl)-1-(4-nitrophenyl)-3-phenyl-1,2,4-triazole Structure

89060-24-2

5-(chloromethyl...

2-phenyl-2-oxazolin-4-one Structure

30216-01-4

2-phenyl-2-oxaz...

~%

5-(chloromethyl)-1-(4-nitrophenyl)-3-phenyl-1,2,4-triazole Structure

89060-24-2

5-(chloromethyl...

4-Nitropheylhydrazine Structure

100-16-3

4-Nitropheylhyd...

~%

5-(chloromethyl)-1-(4-nitrophenyl)-3-phenyl-1,2,4-triazole Structure

89060-24-2

5-(chloromethyl...

2,5-diphenyl-1,2,4-triazole-3-carbaldehyde Structure

89060-38-8

2,5-diphenyl-1,...

Acetophenone Structure

98-86-2

Acetophenone

~85%

3-(2,5-diphenyl-1,2,4-triazol-3-yl)-1-phenylprop-2-en-1-one Structure

89060-66-2

3-(2,5-diphenyl...

2-phenyl-2-oxazolin-4-one Structure

30216-01-4

2-phenyl-2-oxaz...

~%

3-(2,5-diphenyl-1,2,4-triazol-3-yl)-1-phenylprop-2-en-1-one Structure

89060-66-2

3-(2,5-diphenyl...

Phenylhydrazine Structure

100-63-0

Phenylhydrazine

~%

3-(2,5-diphenyl-1,2,4-triazol-3-yl)-1-phenylprop-2-en-1-one Structure

89060-66-2

3-(2,5-diphenyl...

(1,3-diphenyl-1H-1,2,4-triazol-5-yl)methanol Structure

26254-07-9

(1,3-diphenyl-1...

~%

3-(2,5-diphenyl-1,2,4-triazol-3-yl)-1-phenylprop-2-en-1-one Structure

89060-66-2

3-(2,5-diphenyl...

2-phenyl-2-oxazolin-4-one Structure

30216-01-4

2-phenyl-2-oxaz...

~%

1-[(2-methyl-5-phenyl-1,2,4-triazol-3-yl)methyl]piperidine Structure

89060-68-4

1-[(2-methyl-5-...

(2-methyl-5-phenyl-2H-[1,2,4]triazol-3-yl)-methanol Structure

26254-08-0

(2-methyl-5-phe...

~%

1-[(2-methyl-5-phenyl-1,2,4-triazol-3-yl)methyl]piperidine Structure

89060-68-4

1-[(2-methyl-5-...

N/A Structure

26254-15-9

N/A

~%

1-[(2-methyl-5-phenyl-1,2,4-triazol-3-yl)methyl]piperidine Structure

89060-68-4

1-[(2-methyl-5-...

Piperidine Structure

110-89-4

Piperidine

1-Methyl-3-phenyl-1H-1,2,4-triazole-5-carbaldehyde Structure

89060-36-6

1-Methyl-3-phen...

~%

1-[(2-methyl-5-phenyl-1,2,4-triazol-3-yl)methyl]piperidine Structure

89060-68-4

1-[(2-methyl-5-...

(2-methyl-5-phenyl-2H-[1,2,4]triazol-3-yl)-methanol Structure

26254-08-0

(2-methyl-5-phe...

~88%

1-Methyl-3-phenyl-1H-1,2,4-triazole-5-carbaldehyde Structure

89060-36-6

1-Methyl-3-phen...

N/A Structure

89060-51-5

N/A

2-phenyl-2-oxazolin-4-one Structure

30216-01-4

2-phenyl-2-oxaz...

~%

1-Methyl-3-phenyl-1H-1,2,4-triazole-5-carbaldehyde Structure

89060-36-6

1-Methyl-3-phen...

N/A Structure

26254-15-9

N/A

~%

1-Methyl-3-phenyl-1H-1,2,4-triazole-5-carbaldehyde Structure

89060-36-6

1-Methyl-3-phen...

(1-Benzyl-3-phenyl-1,2,4-triazol-5-yl)methanol Structure

26254-20-6

(1-Benzyl-3-phe...

~89%

2-benzyl-5-phenyl-1,2,4-triazole-3-carbaldehyde Structure

89060-37-7

2-benzyl-5-phen...

2-phenyl-2-oxazolin-4-one Structure

30216-01-4

2-phenyl-2-oxaz...

~%

2-benzyl-5-phenyl-1,2,4-triazole-3-carbaldehyde Structure

89060-37-7

2-benzyl-5-phen...

Benzylhydrazine Structure

555-96-4

Benzylhydrazine

~%

2-benzyl-5-phenyl-1,2,4-triazole-3-carbaldehyde Structure

89060-37-7

2-benzyl-5-phen...

Malonic acid Structure

141-82-2

Malonic acid

2,5-diphenyl-1,2,4-triazole-3-carbaldehyde Structure

89060-38-8

2,5-diphenyl-1,...

~97%

3-(2,5-diphenyl-1,2,4-triazol-3-yl)prop-2-enoic acid Structure

89060-70-8

3-(2,5-diphenyl...

2-phenyl-2-oxazolin-4-one Structure

30216-01-4

2-phenyl-2-oxaz...

~%

3-(2,5-diphenyl-1,2,4-triazol-3-yl)prop-2-enoic acid Structure

89060-70-8

3-(2,5-diphenyl...

Phenylhydrazine Structure

100-63-0

Phenylhydrazine

~%

3-(2,5-diphenyl-1,2,4-triazol-3-yl)prop-2-enoic acid Structure

89060-70-8

3-(2,5-diphenyl...

(1,3-diphenyl-1H-1,2,4-triazol-5-yl)methanol Structure

26254-07-9

(1,3-diphenyl-1...

~%

3-(2,5-diphenyl-1,2,4-triazol-3-yl)prop-2-enoic acid Structure

89060-70-8

3-(2,5-diphenyl...

2-phenyl-2-oxazolin-4-one Structure

30216-01-4

2-phenyl-2-oxaz...

~%

1-[(2,5-diphenyl-1,2,4-triazol-3-yl)-piperidin-1-ylmethyl]piperidine Structure

89060-78-6

1-[(2,5-dipheny...

Phenylhydrazine Structure

100-63-0

Phenylhydrazine

~%

1-[(2,5-diphenyl-1,2,4-triazol-3-yl)-piperidin-1-ylmethyl]piperidine Structure

89060-78-6

1-[(2,5-dipheny...

(1,3-diphenyl-1H-1,2,4-triazol-5-yl)methanol Structure

26254-07-9

(1,3-diphenyl-1...

~%

1-[(2,5-diphenyl-1,2,4-triazol-3-yl)-piperidin-1-ylmethyl]piperidine Structure

89060-78-6

1-[(2,5-dipheny...

Piperidine Structure

110-89-4

Piperidine

(2,5-Diphenyl-2H-[1,2,4]triazol-3-yl)-piperidin-1-yl-methanol Structure

89060-77-5

(2,5-Diphenyl-2...

~19%

1,3-diphenyl-1,2,4-triazole Structure

34924-43-1

1,3-diphenyl-1,...

1-[(2,5-diphenyl-1,2,4-triazol-3-yl)-piperidin-1-ylmethyl]piperidine Structure

89060-78-6

1-[(2,5-dipheny...

Piperidine Structure

110-89-4

Piperidine

~%

1-[(2,5-diphenyl-1,2,4-triazol-3-yl)-piperidin-1-ylmethyl]piperidine Structure

89060-78-6

1-[(2,5-dipheny...

2,5-diphenyl-1,2,4-triazole-3-carbaldehyde Structure

89060-38-8

2,5-diphenyl-1,...

~%

1-[(2,5-diphenyl-1,2,4-triazol-3-yl)-piperidin-1-ylmethyl]piperidine Structure

89060-78-6

1-[(2,5-dipheny...

Piperidine Structure

110-89-4

Piperidine

1,5-diphenyl-1,2,4-triazole-3-carbaldehyde Structure

89060-58-2

1,5-diphenyl-1,...

~85%

1-[(1,5-diphenyl-1,2,4-triazol-3-yl)-piperidin-1-ylmethyl]piperidine Structure

89060-79-7

1-[(1,5-dipheny...

1H-1,2,4-Triazole-3-methanol,1,5-diphenyl- Structure

89060-59-3

1H-1,2,4-Triazo...

~%

1-[(1,5-diphenyl-1,2,4-triazol-3-yl)-piperidin-1-ylmethyl]piperidine Structure

89060-79-7

1-[(1,5-dipheny...

3-chloromethyl-1,5-diphenyl-1H-[1,2,4]triazole Structure

26254-13-7

3-chloromethyl-...

~%

1-[(1,5-diphenyl-1,2,4-triazol-3-yl)-piperidin-1-ylmethyl]piperidine Structure

89060-79-7

1-[(1,5-dipheny...

(1,3-diphenyl-1H-1,2,4-triazol-5-yl)methanol Structure

26254-07-9

(1,3-diphenyl-1...

~85%

2,5-diphenyl-1,2,4-triazole-3-carbaldehyde Structure

89060-38-8

2,5-diphenyl-1,...

2-phenyl-2-oxazolin-4-one Structure

30216-01-4

2-phenyl-2-oxaz...

~%

2,5-diphenyl-1,2,4-triazole-3-carbaldehyde Structure

89060-38-8

2,5-diphenyl-1,...

Phenylhydrazine Structure

100-63-0

Phenylhydrazine

~%

2,5-diphenyl-1,2,4-triazole-3-carbaldehyde Structure

89060-38-8

2,5-diphenyl-1,...

[2-(4-methylphenyl)-5-phenyl-1,2,4-triazol-3-yl]methanol Structure

89060-23-1

[2-(4-methylphe...

~81%

2-(4-methylphenyl)-5-phenyl-1,2,4-triazole-3-carbaldehyde Structure

89060-39-9

2-(4-methylphen...

N/A Structure

89060-52-6

N/A

2-phenyl-2-oxazolin-4-one Structure

30216-01-4

2-phenyl-2-oxaz...

~%

2-(4-methylphenyl)-5-phenyl-1,2,4-triazole-3-carbaldehyde Structure

89060-39-9

2-(4-methylphen...

4-Methylphenylhydrazine Structure

539-44-6

4-Methylphenylh...

~%

2-(4-methylphenyl)-5-phenyl-1,2,4-triazole-3-carbaldehyde Structure

89060-39-9

2-(4-methylphen...

[2-(4-bromo-phenyl)-5-phenyl-2H-[1,2,4]triazol-3-yl]-methanol Structure

26254-21-7

[2-(4-bromo-phe...

~87%

2-(4-bromophenyl)-5-phenyl-1,2,4-triazole-3-carbaldehyde Structure

89060-40-2

2-(4-bromopheny...

2-phenyl-2-oxazolin-4-one Structure

30216-01-4

2-phenyl-2-oxaz...

~%

2-(4-bromophenyl)-5-phenyl-1,2,4-triazole-3-carbaldehyde Structure

89060-40-2

2-(4-bromopheny...

p-Bromophenylhydrazine Structure

589-21-9

p-Bromophenylhy...

~%

2-(4-bromophenyl)-5-phenyl-1,2,4-triazole-3-carbaldehyde Structure

89060-40-2

2-(4-bromopheny...

[2-(4-nitro-phenyl)-5-phenyl-2H-[1,2,4]triazol-3-yl]-methanol Structure

26254-22-8

[2-(4-nitro-phe...

~82%

2-(4-nitrophenyl)-5-phenyl-1,2,4-triazole-3-carbaldehyde Structure

89060-41-3

2-(4-nitropheny...

2-phenyl-2-oxazolin-4-one Structure

30216-01-4

2-phenyl-2-oxaz...

~%

2-(4-nitrophenyl)-5-phenyl-1,2,4-triazole-3-carbaldehyde Structure

89060-41-3

2-(4-nitropheny...

4-Nitropheylhydrazine Structure

100-16-3

4-Nitropheylhyd...

~%

2-(4-nitrophenyl)-5-phenyl-1,2,4-triazole-3-carbaldehyde Structure

89060-41-3

2-(4-nitropheny...

4-(Dimethylamino)-N-((1-(4-nitrophenyl)-3-phenyl-1,2,4-triazol-5-yl)methylen)anilin-N-oxid Structure

89060-33-3

4-(Dimethylamin...

~%

2-(4-nitrophenyl)-5-phenyl-1,2,4-triazole-3-carbaldehyde Structure

89060-41-3

2-(4-nitropheny...

5-(chloromethyl)-1-(4-nitrophenyl)-3-phenyl-1,2,4-triazole Structure

89060-24-2

5-(chloromethyl...

~%

2-(4-nitrophenyl)-5-phenyl-1,2,4-triazole-3-carbaldehyde Structure

89060-41-3

2-(4-nitropheny...

2,5-diphenyl-1,2,4-triazole-3-carbaldehyde Structure

89060-38-8

2,5-diphenyl-1,...

~96%

3-(nitrosomethylidene)-2,5-diphenyl-1H-1,2,4-triazole Structure

89060-49-1

3-(nitrosomethy...

Phenylhydrazine Structure

100-63-0

Phenylhydrazine

~%

3-(nitrosomethylidene)-2,5-diphenyl-1H-1,2,4-triazole Structure

89060-49-1

3-(nitrosomethy...

2-phenyl-2-oxazolin-4-one Structure

30216-01-4

2-phenyl-2-oxaz...

~%

3-(nitrosomethylidene)-2,5-diphenyl-1H-1,2,4-triazole Structure

89060-49-1

3-(nitrosomethy...

(1,3-diphenyl-1H-1,2,4-triazol-5-yl)methanol Structure

26254-07-9

(1,3-diphenyl-1...

~%

3-(nitrosomethylidene)-2,5-diphenyl-1H-1,2,4-triazole Structure

89060-49-1

3-(nitrosomethy...


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