Tris (2-hydroxyethyl) ammonium salts: 2, 8, 9-Trihydroprotatranes

…, AI Albanov, TN Aksamentova, SN Adamovich…

Index: Voronkov; Albanov; Aksamentova; Adamovich; Chipanina; Mirskov; Kochina; Vrazhnov; Litvinov Russian Journal of General Chemistry, 2009 , vol. 79, # 11 p. 2339 - 2346

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Citation Number: 14

Abstract

Abstract New method of synthesis of tris (2-hydroxyethyl) ammonium salts, 2, 8, 9- trihydroprotatranes X-[HN (CH 2 CH 2 OH) 3]+, based on the reaction of tris (2-hydroxyethyl) amine (triethanolamine) with ammonium salts NH 4 X (X= F, Cl, Br, I, NO 3, ClO 4) was developed. 1 H, 13 C, 15 N NMR and IR spectra of these protatranes were investigated, as well as those of their analogs with X= RCH 2 COO (R= H; 2-MeC 6 H 4 O; 2-Me-4ClC 6 H ...