Darstellung neuer vicinaler Tricarbonylverbindungen und einiger ihrer Schwefelanaloga

…, J Voß, S Weinschneider

Index: Malmberg, Wolf-Dieter; Voss, Juergen; Weinschneider, Sabine Liebigs Annalen der Chemie, 1983 , # 10 p. 1694 - 1711

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Citation Number: 5

Abstract

Abstract Durch geeignete Oxidationsreaktionen gelingt die Überführung der Malonamide 4 in Mesoxalamide 5, der Benzoylacetamide 17 in Benzoylglyoxylamide 19 und der Pivaloylacetamide 24 in Pivaloylglyoxylamide 26. Auch Schwefelanaloga von 5, 19 und ...

 Related Synthetic Route
N,N'-dimethyl-N,N'-diphenylpropanediamide Structure

36949-57-2

N,N'-dimethyl-N...

~60%

2-bromo-N,N'-dimethyl-N,N'-diphenylpropanediamide Structure

87898-72-4

2-bromo-N,N'-di...

N-Methylaniline Structure

100-61-8

N-Methylaniline

~%

2-bromo-N,N'-dimethyl-N,N'-diphenylpropanediamide Structure

87898-72-4

2-bromo-N,N'-di...

N,N,N',N'-tetrabenzyl-2-bromopropanediamide Structure

87898-70-2

N,N,N',N'-tetra...

~%

N,N,N',N'-tetrabenzyl-2-sulfanylidenepropanediamide Structure

87898-79-1

N,N,N',N'-tetra...

N,N,N'',N''-TETRABENZYL-MALONAMIDE Structure

87898-62-2

N,N,N'',N''-TET...

~%

N,N,N',N'-tetrabenzyl-2-sulfanylidenepropanediamide Structure

87898-79-1

N,N,N',N'-tetra...

Dibenzylamine Structure

103-49-1

Dibenzylamine

~%

N,N,N',N'-tetrabenzyl-2-sulfanylidenepropanediamide Structure

87898-79-1

N,N,N',N'-tetra...

Diethyl malonate Structure

105-53-3

Diethyl malonate

Dibenzylamine Structure

103-49-1

Dibenzylamine

~77%

N,N,N'',N''-TETRABENZYL-MALONAMIDE Structure

87898-62-2

N,N,N'',N''-TET...

N-Methylbenzylamine Structure

103-67-3

N-Methylbenzylamine

Diethyl malonate Structure

105-53-3

Diethyl malonate

~64%

N,N''-DIBENZYL-N,N''-DIMETHYL-MALONAMIDE Structure

14288-00-7

N,N''-DIBENZYL-...

tetraethylammoniumS-(1,3-bis(dibenzylamino)-1,3-dioxopropan-2-yl) sulfurothioate Structure

87898-76-8

tetraethylammon...

~%

N,N,N',N'-tetrabenzyl-2-sulfanylidenepropanediamide Structure

87898-79-1

N,N,N',N'-tetra...

Ethylpyruvate Structure

617-35-6

Ethylpyruvate

Dimethylamine Structure

124-40-3

Dimethylamine

~%

ethyl 3-(dimethylamino)-2-oxo-3-sulfanylidenepropanoate Structure

87898-81-5

ethyl 3-(dimeth...

Ethylpyruvate Structure

617-35-6

Ethylpyruvate

Dibenzylamine Structure

103-49-1

Dibenzylamine

~%

ethyl 3-(dibenzylamino)-2-oxo-3-sulfanylidenepropanoate Structure

87898-82-6

ethyl 3-(dibenz...

ammonium;thiocyanate Structure

1147550-11-5

ammonium;thiocyanate

2-Brom-N,N-dibenzyl-3-oxo-3-phenylpropanamid Structure

87898-84-8

2-Brom-N,N-dibe...

~85%

[1-(dibenzylamino)-1,3-dioxo-3-phenylpropan-2-yl] thiocyanate Structure

87898-90-6

[1-(dibenzylami...

N,N,N'',N''-TETRABENZYL-MALONAMIDE Structure

87898-62-2

N,N,N'',N''-TET...

~54%

N,N,N',N'-tetrabenzyl-2-oxopropanediamide Structure

87898-63-3

N,N,N',N'-tetra...

Dibenzylamine Structure

103-49-1

Dibenzylamine

~%

N,N,N',N'-tetrabenzyl-2-oxopropanediamide Structure

87898-63-3

N,N,N',N'-tetra...

Methyl 4,4-dimethyl-3-oxopentanoate Structure

55107-14-7

Methyl 4,4-dime...

Dimethylamine Structure

124-40-3

Dimethylamine

~26%

N,N,4,4-tetramethyl-3-oxopentanamide Structure

87898-91-7

N,N,4,4-tetrame...

ethyl 4,4,4-trimethylacetoacetate Structure

17094-34-7

ethyl 4,4,4-tri...

Dibenzylamine Structure

103-49-1

Dibenzylamine

~35%

N,N-dibenzyl-4,4-dimethyl-3-oxopentanamide Structure

87898-92-8

N,N-dibenzyl-4,...

N,N,N',N'-TETRAMETHYLMALONAMIDE Structure

7313-22-6

N,N,N',N'-TETRA...

~48%

N,N,N',N'-tetramethyl-2-oxopropanediamide Structure

60672-20-0

N,N,N',N'-tetra...

N,N,N',N'-tetramethyl-2-oxopropanediamide Structure

60672-20-0

N,N,N',N'-tetra...

~56%

N,N,N',N'-tetramethyl-2-oxopropanedithioamide Structure

60672-24-4

N,N,N',N'-tetra...

N,N,N',N'-tetramethyl-2-oxopropanediamide Structure

60672-20-0

N,N,N',N'-tetra...

~0%

N,N,N',N'-tetramethyl-2-oxopropanedithioamide Structure

60672-24-4

N,N,N',N'-tetra...

3-(dimethylamino)-N,N-dimethyl-2-oxo-3-sulfanylidenepropanamide Structure

87898-66-6

3-(dimethylamin...

N,N,N',N'-TETRAMETHYLMALONAMIDE Structure

7313-22-6

N,N,N',N'-TETRA...

~%

N,N,N',N'-tetramethyl-2-oxopropanedithioamide Structure

60672-24-4

N,N,N',N'-tetra...

Dimethylamine Structure

124-40-3

Dimethylamine

Diethyl malonate Structure

105-53-3

Diethyl malonate

~27%

N,N,N',N'-TETRAMETHYLMALONAMIDE Structure

7313-22-6

N,N,N',N'-TETRA...

N,N''-DIBENZYL-N,N''-DIMETHYL-MALONAMIDE Structure

14288-00-7

N,N''-DIBENZYL-...

~48%

N,N'-dibenzyl-N,N'-dimethyl-2-oxopropanediamide Structure

87898-64-4

N,N'-dibenzyl-N...

N-Methylbenzylamine Structure

103-67-3

N-Methylbenzylamine

~%

N,N'-dibenzyl-N,N'-dimethyl-2-oxopropanediamide Structure

87898-64-4

N,N'-dibenzyl-N...

N,N'-dimethyl-N,N'-diphenylpropanediamide Structure

36949-57-2

N,N'-dimethyl-N...

~49%

N,N'-dimethyl-2-oxo-N,N'-diphenylpropanediamide Structure

87898-65-5

N,N'-dimethyl-2...

N-Methylaniline Structure

100-61-8

N-Methylaniline

~%

N,N'-dimethyl-2-oxo-N,N'-diphenylpropanediamide Structure

87898-65-5

N,N'-dimethyl-2...

ethyl 4,4,4-trimethylacetoacetate Structure

17094-34-7

ethyl 4,4,4-tri...

~6%

ethyl 4,4-dimethyl-2,3-dioxopentanoate Structure

87898-93-9

ethyl 4,4-dimet...

N,N,4,4-tetramethyl-3-oxopentanamide Structure

87898-91-7

N,N,4,4-tetrame...

~9%

N,N,4,4-tetramethyl-2,3-dioxopentanamide Structure

87898-94-0

N,N,4,4-tetrame...

Methyl 4,4-dimethyl-3-oxopentanoate Structure

55107-14-7

Methyl 4,4-dime...

~%

N,N,4,4-tetramethyl-2,3-dioxopentanamide Structure

87898-94-0

N,N,4,4-tetrame...

N,N-dibenzyl-4,4-dimethyl-3-oxopentanamide Structure

87898-92-8

N,N-dibenzyl-4,...

~48%

N,N-dibenzyl-4,4-dimethyl-2,3-dioxopentanamide Structure

87898-95-1

N,N-dibenzyl-4,...

ethyl 4,4,4-trimethylacetoacetate Structure

17094-34-7

ethyl 4,4,4-tri...

~%

N,N-dibenzyl-4,4-dimethyl-2,3-dioxopentanamide Structure

87898-95-1

N,N-dibenzyl-4,...

Dibenzylamine Structure

103-49-1

Dibenzylamine

~%

N,N-dibenzyl-4,4-dimethyl-2,3-dioxopentanamide Structure

87898-95-1

N,N-dibenzyl-4,...

N,N,N',N'-tetramethyl-2-oxopropanediamide Structure

60672-20-0

N,N,N',N'-tetra...

~59%

N,N,N',N'-tetramethyl-2-oxopropanedithioamide Structure

60672-24-4

N,N,N',N'-tetra...

3-(dimethylamino)-N,N-dimethyl-2-oxo-3-sulfanylidenepropanamide Structure

87898-66-6

3-(dimethylamin...

N,N,N',N'-TETRAMETHYLMALONAMIDE Structure

7313-22-6

N,N,N',N'-TETRA...

~%

3-(dimethylamino)-N,N-dimethyl-2-oxo-3-sulfanylidenepropanamide Structure

87898-66-6

3-(dimethylamin...

N,N,N',N'-tetrabenzyl-2-oxopropanediamide Structure

87898-63-3

N,N,N',N'-tetra...

~62%

N,N,N',N'-tetrabenzyl-2-oxopropanedithioamide Structure

87898-68-8

N,N,N',N'-tetra...

N,N,N',N'-Tetrabenzyl-1,2-dithiomesoxalamid Structure

87898-69-9

N,N,N',N'-Tetra...

N,N,N'',N''-TETRABENZYL-MALONAMIDE Structure

87898-62-2

N,N,N'',N''-TET...

~%

N,N,N',N'-tetrabenzyl-2-oxopropanedithioamide Structure

87898-68-8

N,N,N',N'-tetra...

Dibenzylamine Structure

103-49-1

Dibenzylamine

~%

N,N,N',N'-tetrabenzyl-2-oxopropanedithioamide Structure

87898-68-8

N,N,N',N'-tetra...

N,N-dibenzyl-4,4-dimethyl-3-oxopentanamide Structure

87898-92-8

N,N-dibenzyl-4,...

~24%

N,N-dibenzyl-2-bromo-4,4-dimethyl-3-oxopentanamide Structure

87898-96-2

N,N-dibenzyl-2-...

ethyl 4,4,4-trimethylacetoacetate Structure

17094-34-7

ethyl 4,4,4-tri...

~%

N,N-dibenzyl-2-bromo-4,4-dimethyl-3-oxopentanamide Structure

87898-96-2

N,N-dibenzyl-2-...

Dibenzylamine Structure

103-49-1

Dibenzylamine

~%

N,N-dibenzyl-2-bromo-4,4-dimethyl-3-oxopentanamide Structure

87898-96-2

N,N-dibenzyl-2-...

4,4-dimethylpentane-2,3-dione Structure

40898-19-9

4,4-dimethylpen...

Dibenzylamine Structure

103-49-1

Dibenzylamine

~%

N,N-dibenzyl-4,4-dimethyl-2,3-dioxopentanethioamide Structure

87898-97-3

N,N-dibenzyl-4,...

N-Methylaniline Structure

100-61-8

N-Methylaniline

Diethyl malonate Structure

105-53-3

Diethyl malonate

~63%

N,N'-dimethyl-N,N'-diphenylpropanediamide Structure

36949-57-2

N,N'-dimethyl-N...

N,N,N'',N''-TETRABENZYL-MALONAMIDE Structure

87898-62-2

N,N,N'',N''-TET...

~91%

N,N,N',N'-tetrabenzyl-2-bromopropanediamide Structure

87898-70-2

N,N,N',N'-tetra...

Dibenzylamine Structure

103-49-1

Dibenzylamine

~%

N,N,N',N'-tetrabenzyl-2-bromopropanediamide Structure

87898-70-2

N,N,N',N'-tetra...

N,N''-DIBENZYL-N,N''-DIMETHYL-MALONAMIDE Structure

14288-00-7

N,N''-DIBENZYL-...

~78%

N,N'-dibenzyl-2-bromo-N,N'-dimethylpropanediamide Structure

87898-71-3

N,N'-dibenzyl-2...

N-Methylbenzylamine Structure

103-67-3

N-Methylbenzylamine

~%

N,N'-dibenzyl-2-bromo-N,N'-dimethylpropanediamide Structure

87898-71-3

N,N'-dibenzyl-2...


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