e.g. Filippa Pettersson or Cancer Res. 75(6) , 1102-12, (2015) or 10.1002/anie.201600521
Regioselective Addition of Mesitol to a 2, 4-Dichloropyridine
…, R Breitenbach, FJ Urban, AM Stewart, III…
Index: Ruggeri, Sally Gut; Vanderplas, Brian C.; Anderson, Bruce G.; Breitenbach, Ralph; Urban, Frank J.; Stewart III, A. Morgan; Young, Gregory R. Organic Process Research and Development, 2008 , vol. 12, # 3 p. 411 - 413
The regioselectivity of the addition of 2, 4, 6-trimethylphenol to 2, 4-dichloro-3, 6- dimethylpyridine can be controlled by the proper choice of catalyst and solvent. The use of catalytic copper (I) salts and pyridine as solvent results in exclusive addition at C-2. In their absence, a mixture of regioisomers is obtained in which addition at C-4 is dominant.