Tetrahedron

Synthesis of methyl (±)-7-oxo-8-methyl-podocarp-8-en-16-oate

F Fringuelli, V Mancini, A Taticchi

Index: Fringuelli,F. et al. Tetrahedron, 1969 , vol. 25, p. 4249 - 4256

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Citation Number: 10

Abstract

... Unfortunately the reduction of the aromatic ring of IV using the technique of Dryden et al.15 coupled with the "reductive hydrolysis" procedure16 for converting the ester group into the corresponding acid, was unsuccessful. ... Recrystallization from 75% EtOH afforded 47 g of XX (81-5%): mp 152(lit.9 152. 4254 F. FRINGUELLI, V. MANCINI and A. TATICCHI Methyl-methoxybenzoyl chloride (XXI). ...