... The Journal of Organic ... DBU, 69 (98), 24:76 (27:73). Et 3 N, 0, N/A. H 2 SO 4 d, 0, N/A. a Mole percent conversion to 3a + 4a after 23 h at 23 °C, determined by HPLC. Values in parentheses are after an additional 23 h at 70 °C. b Ratio of 3a:4a after 23 h at 23 °C, determined by GC ...