... H. Takahata, H. Okajima, M. Nagata, and T. Yamazaki, Chem. Pharm. ... In the NMR spectrum, the half-width of the N-methyl signal of 7 increased at lower temperature, due to the two 12) H. Takahata, T. Hashizume, and T. Yamazaki, Heterocycles, 12, 1449 (1979). ...