Ritchie? was able to reduce G-methylphenan- volume in wzczio under iiitrogeii. Upoil making alkaline ... After purification by sublimation zn vacuo at 110 ', the prod- ... Anal, Calcd. for C,,H~~K: c, 83.55; H, 9.51; N, ... The picrate was prepared and recrystallized from hot ... Anal. Calcd. for CI ~ H ~ ~ S . C ~ H ? OH ( ~ O ? ) ~ ~ : C, 55.80; 13.14. 5-( p-Diethylaminoethyl) -6-methyl-5,6-dihydrophe- ... ~ ~ ~ i . Calcd. for C~~H~~S~.HCI.~/~ ...