Analytical Chemistry

Carbon-13 and fluorine-19 nuclear magnetic resonance chemical shift studies of carbon-13 enriched p-fluorobenzoyl derivatives

MP Spratt, D Armistead, E Motell, HC Dorn

Index: Spratt, M. P.; Armistead, D.; Motell, E.; Dorn, H. C. Analytical Chemistry, 1985 , vol. 57, # 1 p. 359 - 361

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Citation Number: 2

Abstract

Sir: Recently Dorn and co-workers (I) have reported the use of p-fluorobenzoyl chloride as a 19F NMR tagging reagent for characterizing molecules with active hydrogen functional groups. The base catalyzed reaction of p-fluorobenzoyl chloride has provided a convenient method for" F NMR analysis of alcohols, phenols, carboxylic acids, amines, and thiols. More recently, the p-fluorobenzoyl chloride reagent has been used to characterize biological ...