Preparative Buffered Formolysis of 1-0Ns.-To 30 ml of 0.103 M potassium formate-formic acid solution, which had been prepared and kept in a nitrogen atmosphere, was added 82 mg (0.247 mmol) of 1-ONs. The solution was placed in a constanttemperature bath at 60.00= t 0.05'for 20 hr (approximately 10 tilz). It was then cooled and placed in a separatory funnel with 50 ml of ether. The ether solution was washed with four 20-ml portions of water, two ...
