Abstract Some new (3, 5-aryl/methyl-1H-pyrazol-1-yl)-(5-arylamino-2H-1, 2, 3-triazol-4-yl) methanones were synthesized and characterized by 1 HNMR, 13 C NMR, MS, IR spectra data and elemental analyses or high resolution mass spectra (HRMS). During the procedure, Dimroth rearrangement was used in this synthesis.