A variation in reaction conditions has produced this new compound instead of the 1, 3, 5-tri- p-toluenesulfonylcyclo-trimethylenetriamine reported by McMaster.'To 0.05 mole (7 9.) of hexamethylenetetramine in 80 cc. of water was added 0.199 mole (37.8 g.) of p- toluenesulfonyl chloride. To this stirred solution, covered with 60 cc. ether, was added 53 cc. of a 1570 aqueous sodium hydroxide solution (0.199 mole, 7.95 g. sodium hydroxide) at ...
