Tetrahedron letters

Removal of silyl protecting groups from hydroxyl functions with ammonium fluoride in methanol

W Zhang, MJ Robins

Index: Zhang, Weijian; Robins, Morris J. Tetrahedron Letters, 1992 , vol. 33, # 9 p. 1177 - 1180

Full Text: HTML

Citation Number: 208

Abstract

Tetrahedron Lmrs. Vol. 33. No. 9, pp. 1177-l 180, 1992 Primed in Groat BAain ... REMOVAL OF SILYL PROTECTING GROUPS FROM HYDROXYL FUNCTIONS WITH AMMONIUM FLUORIDE IN METHANOL' ... Department of Chemistry, Brigham Young University, Provo, UT 84602, USA ... Summary: Treatment of silyl ethers with excess ammonium fluoride in methanol at 60 OC effected cleavage to alcohols within 5 hours. Deprotection at ambient temperature required 1-2 ...

~99%

Radical reactions in aqueous medium using (Me3Si) 3SiH

[Postigo, Al; Kopsov, Sergey; Ferreri, Carla; Chatgilialoglu, Chryssostomos Organic Letters, 2007 , vol. 9, # 25 p. 5159 - 5162]

Efficient and catalytic deprotection of triphenylmethyl ethe...

[Khalafi-Nezhad, Ali; Fareghi Alamdari, Reza Tetrahedron, 2001 , vol. 57, # 31 p. 6805 - 6807]

Lactobacillus reuteri 2′-deoxyribosyltransferase, a novel bi...

[Trelles; Fernandez; Lewkowicz; Iribarren; Sinisterra Tetrahedron Letters, 2003 , vol. 44, # 12 p. 2605 - 2609]

High-throughput five minute microwave accelerated glycosylat...

[Bookser, Brett C.; Raffaele, Nicholas B. Journal of Organic Chemistry, 2007 , vol. 72, # 1 p. 173 - 179]

A new method for the synthesis of 2′-O-benzyladenosine using...

[Kozai, Shigetada; Fuzikawa, Tomoyo; Harumoto, Keisuke; Maruyama, Tokumi Nucleosides, Nucleotides and Nucleic Acids, 2003 , vol. 22, # 2 p. 145 - 151]